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NMR Spectroscopy Quiz | NMR Spectroscopy Objective Type Questions and Answers

(21) NMR spectroscopy indicates the chemical nature of the __________ and spatial positions of _______
[A] Electrons, Protons
[B] Neutrons, electrons
[C] Nuclei, electrons
[D] Nuclei, neighbouring nuclei
Answer: Nuclei, neighbouring nuclei
(22) When energy is absorbed by the sample, the absorption can be observed as a change in signal developed by which of the following components?
[A] Amplifier
[B] Photodetector
[C] GM counter
[D] Radiofrequency detector
Answer: Radiofrequency detector

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(23) Which of the following are considered to be the lowest form of Electromagnetic radiation?
[A] IR radiation
[B] Micro waves
[C] UV radiation
[D] Radio waves
Answer: Radio waves
(24) Nuclei having either the number of protons or neutrons as odd have _______ spin.
[A] Integral spin
[B] Half integral spin
[C] Zero spin
[D] Positive spin
Answer: Half integral spin
(25) The difference between the field necessary for resonance in the sample and in some arbitrary chosen compound is which of the following?
[A] Field shift
[B] Matrix effects
[C] Chemical shift
[D] Resonance shift
Answer: Matrix effects
(26) Which of the following organic compound with molecular formula C3H C12 exhibits only one signal in the IH NMR spectrum?
[A] 2, 2-dichloropropane
[B] 1, 2-dichloropropane
[C] 1, 3-dichloropropane
[D] 1, 1-dichloropropane
Answer: 2, 2-dichloropropane
(27) The 1H NMR spectrum of CH3OCHCICH2Cl will exhibit ________
[A] A three proton doublet. One proton singlet and a two proton doublet
[B] A three proton singlet. One proton singlet and a two proton doublet
[C] A three proton singlet. One proton triplet and a two proton doublet
[D] A three proton triplet. One proton triplet and a two proton triplet
Answer: A three proton singlet. One proton triplet and a two proton doublet
(28) Which of the following 1H-NMR spectrum of compound with molecular formula C4H9NO2 shows delta 5.30 (broad, IH), 4.10(q, 2H), 2.80 (d, 3H), 1.20 (t, 3H) ppm?
[A] CH3NHCOOCH2CH3
[B] CH3CH2NHCOOCH3
[C] CH3OCH2CONHCH3
[D] CH3CH2OCH2CONH2
Answer: CH3NHCOOCH2CH3
(29) Which of the following has three types of hydrogens in the following compounds?
[A] Br-CH = CH2
[B] CH3 – CH2 – CH3
[C] C6H5CH2
[D] CH3– CH2 – CH(CH3) – N02
Answer: Br-CH = CH2
(30) Which of the compound show only one signal is present in the PMR spectra ?
[A] C3H4, C3H6
[B] C4H6, C5H12
[C] C8H18, C2H6O
[D] All of the mentioned
Answer: All of the mentioned
31 How many Hertz does 1 ppm correspond to for an PMR spectrometer operating at a radio frequency of 60 MHz and 100 MHz?
[A] 6 Hz, 10 Hz
[B] 60 Hz, 100 Hz
[C] 100 Hz, 60 Hz
[D] 10Hz, 100Hz
Answer: 60 Hz, 100 Hz
32 Compound C4H10O gave PMR spectrum consisting of two groups of lines (multiplets) with relative intensities in the ratio 3 : 2. Other compound of the same formula exhibited two lines with relative area of 9 : 1. What are these compounds.
[A] Diethyl ether and n-butanol
[B] t-Butyl alcohol and 1-Methoxypropane
[C] diethyl ether and t-Butyl alcohol
[D] Diethyl ether and 2-Methoxypropane
Answer: diethyl ether and t-Butyl alcohol
33 A proton Hb is coupled to four equivalent protons Ha. The multiplicity and the relative intensity of lines in the signal Hb is
[A] Doublet, I : 4
[B] Triplet, I : 4 : 6
[C] Quintet, 1 : 4 : 6 : 4 : 1
[D] Quartet, 1 : 4 : 6 : 4
Answer: Quintet, 1 : 4 : 6 : 4 : 1
34 NMR spectroscopy indicates the chemical nature of the __________ and spatial positions of _______
[A] Electrons, Protons
[B] Neutrons, electrons
[C] Nuclei, electrons
[D] Nuclei, neighbouring nuclei
Answer: Nuclei, neighbouring nuclei
35 Interaction between matter and electromagnetic radiation can be observed by subjecting a substance to magnetic fields in which of the following manner?
[A] Both fields should be stationary
[B] Both fields should be varying
[C] One field should be stationary and the other should be varying
[D] It must be subjected to only one field
Answer: One field should be stationary and the other should be varying
36 When energy is absorbed by the sample, the absorption can be observed as a change in signal developed by which of the following components?
[A] Amplifier
[B] Photodetector
[C] GM counter
[D] Radiofrequency detector
Answer: Radiofrequency detector
37 Which of the following are considered to be the lowest form of Electromagnetic radiation?
[A] IR radiation
[B] Micro waves
[C] UV radiation
[D] Radio waves
Answer: Radio waves
38 The amount of energy available in radio frequency radiation is sufficient for which of the following?
[A] Excite an atom
[B] Vibrate an atom
[C] Vibrate a molecule
[D] Affect the nuclear spin of an atom
Answer: Affect the nuclear spin of an atom
39 When placed in a magnetic field, all the random spins of the nuclei
[A] stop
[B] reverse direction
[C] align with the magnetic field
[D] rotate to 90° away from the induced field
Answer: align with the magnetic field

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